AN IMPROVED METHOD FOR SIMULTANEOUS DETERMINATION OF EXCHANGEABLE BODY SODIUM AND POTASSIUM

IMPROVED CHROMATOGRAPHIC METHOD FOR DETERMINATION OF SODIUM DICLOFENAC IN INJECTABLE SOLUTION AND PREDICTION OF CHEMICAL STABILITY

Two modified methods for assaying sodium diclofenac were developed by GC and HPLC. Diclofenac was converted into methyl ester derivative by methyl iodide in acetone. The ester was extract and subjected to GLC with flame ionization detector. %5 SE-30/chrom W-HP (80-100 mesh) was used as a column in GC. For reversed phase HPLC, the mobile phase was methanol and water (55-45). The separation was p...

[Total exchangeable sodium, exchangeable potassium and total body water in some endocrine diseases].

概要 諸種 内分 泌疾患 々者についてtotal exchangeable sodium (Nae)お よびpotassium (Ke)を 測定 し,得 た成績 をtotal body water (TBW)か ら算出 したlean body massと の関連 において比較 した. 原発性 アル ドス テロ ン症ではNaeは 著増 し, Keは 減少 していた.一 方続発性 アル ドステ ロン症を伴な つた腎尿 細管 性 アシ ドージスでは, Naeお よびTBWの 増加は な くKeは 著減 していた. Cushing症 候 群 ではKeは 減少 していた. Addison病 では予想 されたNaeの 減少, Keの 増加 はみ られなかつた.褐 色 細胞腫 ではNae, Keお よびTBWは いずれ も正常 であつた.甲 状線機能亢 進症 ではNae増 加, Ke減 少 の傾 ...

An improved HPLC method for determination of colocynthin in colocynth

Background and objectives: Colocynthin is the major active secondary metabolite of colocynth, Citrullus colocynthis (L.) Schrad, which has been used in traditional and ethno medicine of many countries.  It could be considered as an active marker for quality control of colocynth and its herbal products. Analysis and standardization of colocynth and its herbal preparations are a critical...

Equations for the prediction of normal values for exchangeable sodium, exchangeable potassium, extracellular fluid volume, and total body water.

Despite the valuable research information on body electrolytes and water that is gained from isotope dilution studies, these investigations have not become routine clinical procedure. This is partly due to the fact that normal ranges for exchangeable sodium (NaE), exchangeable potassium (KE), extracellular fluid volume (E.C.F.V.), and total body water (T.B.W.) are wide owing to great individual...

Interrelations between total exchangeable sodium, potassium, body water, and serum sodium and potassium concentrations in hyponatremic and normonatremic heart disease.